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Mon Dec 29 20:06:11 2008 

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Experimental Composite Propellant
P. O. Box 1414
Murray, KY 42071
 
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(Contributed - by [Featured Reviewer] Dick Stafford - 04/01/02[Author's Home Page])

Brief:
For some time, I've been interested in learning how to make composite motors and have heard many recommendations for 'Pr'fesser' Terry McCreary's book, "Experimental Composite Propellant." When I discovered that Aerocon distributes the book, I couldn't resist ordering a copy. I thoroughly enjoyed the book and it was worth the price just to learn more about those cool little things that I love to stuff into my rockets. This review provides an overview of the book rather than a technical critique, as I'm just a beginner in this field.

Overview:
The book is informally bound and self-published. It includes a 3 1/2" disk (Excel or Quattro Pro format) with the ProPel design spreadsheets (more about this later) and a nifty executable that provides a tutorial on how rocket motors work, called 'Motortut'. The other program referenced in the text, PropEP, is not provided, but there are references on where to get it online (it's also free).

This book falls somewhere between a cookbook, lecture notes, and a textbook. It is written in an easy to read, informal format and is non-technical. That is, the author provides just enough theory to let you know what you are doing and why. After some compulsory disclaimers, introductions and acknowledgements, he gets down to business. The first meaty section is entitled "Safety First" - a very prudent starting point. It includes dos and don'ts, and a proposed safety code. In the following section, he discusses the legality of propellant making. He presents guidelines to stay legal, making sure you realize that it is up to you to ensure your compliance with not only federal, but also state and local laws as well.

Next comes some background on composite propellant and a description of how a composite motor works. This is pretty basic stuff but is necessary for completeness. The Motortut program provides a nice graphical description of much of this material. Put this on a PC with a projector and you're ready to teach a scout troop about rocket motors.

Rocket PicThe subsequent sections provide some light theory, covering: motor thrust, specific impulse (Isp), total impulse, burn rate, chamber pressure, and burn profiles (neutral, progressive, and regressive). He defines the area ratio (Kn), which equals the area of burning propellant surface divided by the area of the nozzle throat. It turns out this parameter is directly related to chamber pressure and provides the basis for, among other things, the control of burn characteristics and the scaling of a motor design. He continues by describing different grain configurations (gee, I now understand what a Bates grain really is!) and nozzle design.

He then moves on to more hands-on stuff, describing in detail all the equipment and supplies you will need. These items are broken down into 'gotta have', 'nice to get later' and 'for vacuum processing' categories. This is followed by a simple propellant formula with a step-by-step, 'cookbook' process for making enough propellant for several G motors. One thing to note is that his propellant descriptions are based on using PBAN as the binder. I personally haven't formed an opinion about whether PBAN is better than HTPB, which in my limited perspective seems more commonly used. He does provide enough information to use HTPB, but it would take a tad more effort from the novice.

Being a scientist, the Pr'fesser stresses keeping a good lab notebook to keep track of your experiments. (We engineers like them too!) He has a section on troubleshooting, one on building static test motors, one on performing the static tests, and one on how to use the data from your tests to characterize your propellant.

Now the focus changes from motor building to motor design. He discusses design parameters and a design procedure. Several examples of adapting his basic propellant for different motor sizes are provided. Then, he discusses subjects like oxidizer particle size, the effects of metals, burn rate modifiers, etc. Several propellant variations are provided, along with their characterizations. Finally, he ends the main body of the book with a discussion of scaling.

But that's not it. Over half of the book's 243 pages are in the appendices.

Excel

The appendices include a description of the PropEP program and the author's ProPel notebook. In my case, the latter includes several spreadsheets within an Excel Workbook. I included a screen snap of one of the ProPel sheets, which allows you to compute either nozzle throat size or Kn given the grain dimensions. He continues with the plans for a curing oven, the use of coring rods, nozzle construction (here you really need machining skills), the design and construction of reloadable motors (ack, more machining), and scratch building igniters (I like both Igniterman and Magnelite). He goes on to give an overview of polymer chemistry, describing the reactions between binders, curatives, crosslinkers, bonding agents, catalysts, plasticizers, and surfactants. This all leads to a description and examples of curing calculations. Next are sections on mixing HTPB, how to do machine mixing (the basic procedure uses hand mixing), vacuum processing, building an instrumented thrust stand, and a description of the combustion process. There also is a lengthy vendor list (chemicals and equipment) and an annotated bibliography including both books and on-line resources. He concludes the book with a miscellaneous set of essays that he calls 'Sermonettes.' Well, I am worn out and leave it up to you to get the book and see what's in this final section.

Summary:
This is a fascinating book and I think most rocketeers would enjoy it, even if you do not plan to build motors. I have no doubt that I learned enough to make a composite motor. However, the book clearly taught me one thing that I had already suspected. That is, making motors can be *relatively* safe, but is by no means risk free. It is an activity that is not to be taken lightly and one does NOT want to cut corners, as your safety and the safety of others is at stake. And for now, I just don't have an adequate location to make them. Being new to this stuff, the only other thing I'd like to see in the book is expanded treatment of HTPB, including a cookbook example of a basic propellant (again, it seems that most people I'm familiar with use this binder), and some sample propellant formulations with their characterizations. Anyone with any experience will probably think this is too much spoon-feeding.

I rate this book a '5'. To quote the Pr'fesser, "more knowledge is almost always better."

Overall Rating: 5 out of 5


Experimental Composite Propellant, The Book review is provided courtesy of:
Rocket Pic

Picture of the book cover. I've already got tabs placed on the pages I've flipped to more than once. I've only had it a little less than a week now....
The other day, I forwarded Darrell some information about Pr'fessor Terry McCreary's recently self-published book "Experimental Composite Propellant." To be honest, I thought I had talked about the book enough in the forums, etc., but that it might be of value posting the information about procurement and a description where everyone could see it for awhile. Well, I guess Darrell wasn't satisfied with that, so he asked me to do a critical review of the book as a service to fellow "Research" rocketeers selecting a good "Introduction to" experimental rocketry book. As always... I've never been shy or short of words, so I'm happy to oblige as follows.


Some basic concepts of composite propellant and grain architecture are discussed.
To be quite honest, there is not a huge amount of information in "Experimental Composite Propellant" which is not available in other publications. You'll note the author frequently references research material, as any well studied academic should (why re-invent the wheel?). So, what makes this book special? It compiles information from more than a dozen resources, digests it, and presents the text in a way no other popular publication has; specifically for the amateur rocket scientist.

The 243 page book (initial printing) covers both beginner and advanced topics, providing step-by-step selection of materials for Ammonium Perchlorate composite propellant, motor casing preparation, mixing, casting, testing, and evaluation of the finished product. Additionally, contained are discussions of more advance topics intended to de-mystify the combustion process of a rocket motor, thoroughly explain the properties of applicable chemicals, explain the function of application-specific additives, how variables affect the polymerization process, to name a few of the highlights.


Pictures from a "How to" detailing the mixing and casting of a batch of AP/PBAN composite propellant.
Content also include a thorough list of web-based and hard-copy references and material suppliers, as well as appendices covering everything from selection of additives to a "Sermonette" explaining why making your own rocket motors WILL NOT likely save you money in the long run.


The 106 page appendix is nearly half of the book! Good Grief Pr'fessor, where did you find all of this great information?(!)
Delivered with "Experimental Composite Propellant" is a 3.5" floppy disk with several useful utilities. PropEL is a series of spreadsheets in an Excel or Quattro Pro notebook. Spreadsheets included are used to accurately model Bates grain motors, calculate 'a' and 'n' (given supplied variables), 'Kn', volume of a coring rod, volume of a given motor design, and more. PropEL, to say it simply, is "designed to make propellant and motor calculations easier," to quote the introduction of software from the book (with the Pr'fessor's permission....). PropEP is also included, a freeware program used to evaluate useful raw propellant parameter. Instructions for use and explanation of output are well documented for all provided software. These are very powerful tools to the serious research rocketeer.

In short, this book is written to help the entry-level rocket scientist successfully get off the ground, and for the Journeyman to advance his knowledge of this fairly narrow topic. Of course, the guidance of an experienced research rocketeer is still highly recommended for anyone interested in working with the materials and formulas contained therein.

Jeers: Written like a friend standing over your shoulder, helping you understand the significant dangers and the way to avoid them. The pace and content of the book allows for quick success.

Sneers: In my very subjective opinion (that should read EXTREMELY subjective opinion), I would like to see more HTPB bound composite step-by-step content. There is a significant amount of detail in the chapter-text about HTPB, the additives, and how to select a proper amount of curative for a given composition, but I would prefer to see one chapter dedicated to PBAN composites, and one to HTPB composites. The reasons the Pr'fessor prefers the PBAN route are well documented in the book, so once again, it is not an issue, just a subjective opinion. My first successful experiences were with HTPB binder, so it may just be an old romance I can't quite get out of my heart.

Editor's Note:

A section detailing proper curing catalyst ratios for the common binder types.
Recently, Sue McMurray of TMT was so pleased with the contents of this book that she recommended it be adopted as the introductory manual for the Tripoli Experimental program. Her email stated:
"I have just finished a quick read through Professor Terry McCreary's new book, 'Experimental Composite Propellant'. Terry's book is a landmark in the field of experimental solid propellant motors, and I've read them all (and had to do the problems at the end of each chapter in Sutton).

'Experimental Composite Propellant' is safe, sane, complete and comprehensive. I highly recommend it for ALL hobby rocketeers. You need to know how your motors actually work to utilize the technology more efficiently and Terry makes it easy to understand. No scary integrals or differential equations, just high school math. And, the chapters and sections on safety were obviously written after years of teaching Frosh Chem 101 labs.

I would like to recommend to the TRA BOD that this book be adopted as the introductory manual for Tripoli Experimental. TMT is keeping our copy right here, first book on the shelf. Sutton, move over."

Sincerely,
Sue McMurray
TMT Chair

Details of constructing and operating PC-based static test stand.
What you've all been waiting for. Instructions from The Pr'fessor to obtain a copy:

DISCLAIMER (mandatory)

To obtain the special introductory price on ECP, print, fill out, and sign this form, and include:
  • A money order for $39 US plus s/h (3.25 US, $7 Canada, $9 elsewhere)
  • A clear photocopy of a driver's license, passport, or other identification showing that you are 21 years of age or older (photo, birthdate, address must be clearly visible).
This will be kept on file. Please note:
  • Incomplete orders will not be processed.
  • Select disk format: Quattro Pro or Excel
  • The undersigned hereby acknowledges and affirms that:
    1. no warranty of any sort is provided for, or is implied by, the product(s) being ordered from the seller.
    2. the undersigned assumes all responsibility for the use and for the consequences of use of the product(s).
    3. the undersigned will not use the product(s) in violation of any federal, state, or local law.
    4. the undersigned holds the seller and/or author of the product(s) blameless and harmless for any and all actions of the user of the product(s).
    5. the undersigned holds the seller and/or author of the product(s) blameless and harmless for any and all consequences of the actions of the user of the product(s).
Signed__________________________________________________________

Print Name______________________________________________________

Address________________________________________________________

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Date____________________________________________________________

**Personal checks will be accepted only at the full list price of $55.95 plus s/h, and will be held until the check clears.

Mail to:
Experimental Rocketry Group
P. O. Box 1414
Murray, KY 42071

Written and submitted by Chuck Andrus for Rocketry Online -- Copyright 1996-2000

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